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    The vial transfer mechanism is movable in x y and z directions to capture and move a selected vial The autosampler has a series of valves operable under central control to selectively introduce two different standards into the sample and after obtaining the sample for rinsing and purging the conduits or lines and needles to reduce sample

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    Place the vials in a controlled rate freezing unit From room temperature cool at 1 C/min to 40 C If the freezing unit can compensate for the heat of fusion maintain rate at 1 C/min through the heat of fusion At 40 C plunge into liquid nitrogen Alternatively place the vials in a Nalgene 1 C freezing apparatus

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